| 引用本文: | 盘毅,胡芸,宋威.二酚基甲烷的合成与表征.[J].国防科技大学学报,2005,27(2):15-19.[点击复制] |
| PAN Yi,HU Yun,SONG wei.The Synthesis and Characterization of Bi-phenolic Methane[J].Journal of National University of Defense Technology,2005,27(2):15-19[点击复制] |
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| 二酚基甲烷的合成与表征 |
| 盘毅1, 胡芸1, 宋威2 |
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(1.国防科技大学 航天与材料工程学院，湖南 长沙 410073;2.四川亭江科技股份有限公司，四川 什邡 610025)
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| 摘要: |
| 利用正交实验，研究了苯酚和甲醛在酸性催化剂的作用下合成二酚基甲烷的反应。探讨了合成各条件对产物的收率、双核比例的影响，并对产物的分子量、熔点、双核含量进行了分析表征。 |
| 关键词: 二酚基甲烷 合成 双酚F |
| DOI： |
| 投稿日期：2004-06-22 |
| 基金项目: |
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| The Synthesis and Characterization of Bi-phenolic Methane |
| PAN Yi1, HU Yun1, SONG wei2 |
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(1.College of Aerospace and Materials Engineering, National Univ. of Defense Technology, Changsha 410073, China;2.Sichuan Tingjiang Science and Technology Stock Company, Shifang 610025, China)
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| Abstract: |
| Bi-phenolic methane is synthesized by the reaction of phenol and formaldehyde solution in the presence of acid catalyst. Through orthogonal design experiments, the effective regularities of synthetic conditions on the yield rate and bi-nucleus ratio of bi-phenolic methane are discussed. The properties of bi-phenolic methane, such as molecular weight, melting point and bi-nucleus ratio are analyzed and their characteristics expounded. |
| Keywords: bi-phenolic methane synthesis bi-phenol F |
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