The paper introduces a new synthetic method for molybdenum bronze NaxMo6O17 by solid phase reaction. It has been prepared from stoichiometric mixture MoO3 and MaI,or Na2C2O4 in N2 atmosphere at high temperatures. The method for composition and thermal analysis is also discussed in it.
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王本根,原培胜.新的固相反应法合成钼青铜化合物 NaxMo6O17的研究[J].国防科技大学学报,1991,13(4):79-82. Wang Bengen, Yuan Peisheng. A New Synthetic Method for Molybdenum Bronze NaxMo6O17 by Solid Phase Reaction[J]. Journal of National University of Defense Technology,1991,13(4):79-82.