| 引用本文: | 张学骜,龙永福,许静,等.5－乙酰基－2－氨基二苯甲酮的合成.[J].国防科技大学学报,2003,25(5):31-35.[点击复制] |
| ZHANG XueAo,LONG YongFu,XU Jing,et al.Synthesis of 5-Acetyl-2-aminobenzophenone[J].Journal of National University of Defense Technology,2003,25(5):31-35[点击复制] |
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| 5－乙酰基－2－氨基二苯甲酮的合成 |
| 张学骜, 龙永福, 许静, 谢凯, 安立华 |
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(国防科技大学 航天与材料工程学院，湖南 长沙 410073)
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| 摘要: |
| 用对硝基苯乙酮、乙二醇、苯乙腈、氢气、高氯酸为原料，经酮基保护，环化，催化加氢和消除反应，合成出较高产率的5-乙酰基-2-氨基二苯甲酮。对反应机理作了初步探讨，并用元素分析、IR和1HNMR对其结构进行了表征。 |
| 关键词: 5－乙酰基－2－氨基二苯甲酮 合成 表征 |
| DOI： |
| 投稿日期：2003-03-18 |
| 基金项目:国家部委基金资助项目(51307) |
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| Synthesis of 5-Acetyl-2-aminobenzophenone |
| ZHANG XueAo, LONG YongFu, XU Jing, XIE Kai, AN LiHua |
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(College of Aerospace and Materials Engineering, National Univ. of Defense Technology, Changsha 410073, China)
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| Abstract: |
| The 5-acetyl-2-aminobenzophenone with high yield was synthesized by using p-nitroacetophenone, ethylene glycol, phenylacetonitrile, hydrogen, perchloric acid as raw materials. The reaction mechanism is discussed simply, and the structure of compound is identified by elemental analysis, IR and 1HNMR. |
| Keywords: 5-acetyl-2-aminobenzophenone synthesis characteristic |
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