| 引用本文: | 王清华,王本根,徐艳,等.Sol-gel-水热法合成Li快离子导体无机纳米粉.[J].国防科技大学学报,2005,27(5):113-116.[点击复制] |
| WANG Qinghua,WANG Bengen,XU Yan,et al.The Preparation of Lithium Fast Ionic Conductor by Sol-Gel-Hydrothermal Method[J].Journal of National University of Defense Technology,2005,27(5):113-116[点击复制] |
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| Sol-gel-水热法合成Li快离子导体无机纳米粉 |
| 王清华, 王本根, 徐艳, 刘宏宇 |
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(国防科技大学 航天与材料工程学院，湖南 长沙 410073)
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| 摘要: |
| 利用sol-gel-水热法合成Li快离子导体无机纳米粉。探讨了分散剂、碱含量及煅烧温度对纳米粉表面形貌和电导率的影响。以聚乙二醇12000为分散剂、碱含量为总体系的1.0%，在350℃煅烧的工艺条件下，合成了室温电导率达2.59×10-3S?cm-1的Li快离子导体无机纳米粉。 |
| 关键词: Li快离子导体 无机纳米粉 sol-gel-水热法 |
| DOI： |
| 投稿日期：2005-06-29 |
| 基金项目:国家部委基金资助项目（51412010101KG01） |
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| The Preparation of Lithium Fast Ionic Conductor by Sol-Gel-Hydrothermal Method |
| WANG Qinghua, WANG Bengen, XU Yan, LIU Hongyu |
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(College of Aerospace and Materials Engineering，National Univ.of Defense Technology，Changsha 410073，China)
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| Abstract: |
| The solid fast ionic conductors are synthesized by sol-gel-hydrothermal method. The influences of the dispersion reagent, the mass of alkalinity and the temperature of calcinations on the surface description of nanometer-powder and electric conductivity are discussed. When PEG 12000 is used as dispersion reagent,the mass of alkalinity is 1.0%,the temperature of calcinations is 350℃, and the electric conductivity of Lithium Fast Ionic Conductor synthesized at the room temperature is 2.59×10-3S?cm-1. |
| Keywords: lithium fast ionic conductors inorganic nanometer-powder sol-gel-hydrothermal method |
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