A process was studied to make continuous silicon carbide fiber from polycarbosilane (PC) served as precursor. The manufacture process includes the synthesis of PC,and melt spinning in an equipment with a nozzle of 100 holes to produce 10-15μm diameter fibers. These fibers were cured single ply yarn, and were coutinuously pyrolyzed to 1200℃ in an inert environment. They then undergo siziug,dry and drum reel to produce amorphous high performance ceramic fiber. The fibers have a tansile strength of 2-2.3GPa and an elastic moduli of 178GPa. Their length>100m. The effect between structure and properties of SiC fiber made by various technical parameters has been studied in this paper.
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Feng Chunxiang, Liu Xinwei, Yang Yiming, Lu Yi, Song Yongcai, Lei Shaozeng. Preparation of Continuous Silicon carbide Fiber[J]. Journal of National University of Defense Technology,1993,15(1):66-72.